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投稿时间：2011-03-31 修订日期：2011-04-28
投稿时间：2011-03-31 修订日期：2011-04-28
中文摘要: 应用波长扫描X射线荧光光谱法对中低合金钢、电工钢、高锰钢、不锈钢中锰元素进行测定。采用经验系数法校正元素间的增强－吸收效应和光谱重叠干扰，元素检测限为2.1 μg/g，线性相关系数大于0.9998。考察分析方法的精密度和准确度,元素的测定结果与认定值一致，相对标准偏差小于2%。
Abstract:Manganese elements in low alloy steel, electrician steel, high manganese steel and stainless steel were measured with sequential wavelength scanning X-ray fluorescence spectrometry. Interferences due to absorption enhancement and spectral overlapping between the elements were corrected by the empirical factor method. The detection limit of manganese element is 2.1μg/g and linear correlation coefficients is more than 0.9998. The accuracy and precision of this method were studied. The results are consistent with the certified values and have relative standard deviation of less than 2%.
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引用文本：
邓军华,曲月华,王一凌.X射线荧光光谱法快速测定钢基中锰元素含量[J].中国无机分析化学,2011,1(2):63-65.
DENG Junhua,QU Yuehua,WANG Yiling.Rapid Quantitative Determination of Manganese Element in Steel by X-ray Fluorescence Spectrometry[J].Chinese Journal of Inorganic Analytical Chemistry,2011,1(2):63-65.
邓军华,曲月华,王一凌.X射线荧光光谱法快速测定钢基中锰元素含量[J].中国无机分析化学,2011,1(2):63-65.
DENG Junhua,QU Yuehua,WANG Yiling.Rapid Quantitative Determination of Manganese Element in Steel by X-ray Fluorescence Spectrometry[J].Chinese Journal of Inorganic Analytical Chemistry,2011,1(2):63-65.
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