本文已被:浏览 1548次 下载 1710次
投稿时间:2019-04-28 修订日期:2019-09-11
投稿时间:2019-04-28 修订日期:2019-09-11
中文摘要: 建立了一套快速准确测定低品位铬铁矿中Cr的分析方法。通过采用浓硝酸-硫磷混酸对试样进行消解,利用电感耦合等离子体发射光谱仪(ICP-OES)测定低品位铬铁矿中Cr。该方法检出限低,测定范围广,线性范围内相关系数R为0.999911,相对标准偏差在1.99-6.00%、回收率在96.8%-104.8%间,方法对比数据吻合,结果满意,适宜推广。
中文关键词: ICP-OES 铬铁矿 Cr
Abstract:A set of analytical methods for rapid and accurate determination of Cr in low-grade chromite ore was established. After the sample was digested by concentrated nitric acid-sulfur phosphorous mixed acid, Cr in low-grade chromite ore was determined by inductively coupled plasma optical emission spectrometry. The detection limit of this method is low, and the measurement range is wide. The correlation coefficient R in the linear range is 0.999911.The relative standard deviation was 1.99-6.00% and the recovery was between 96.8%-104.8%. The results of the method were consistent and satisfactory. The method is suitable for promotion.
文章编号: 中图分类号: 文献标志码:
基金项目:
作者 | 单位 | |
lanlvdeng* | 湖北冶金地质研究所 | 874207609@qq.com |
Author Name | Affiliation | |
lanlvdeng | CENTRAL SOUTH INSTITUTE OF METALLURGICAL GEOLOGY | 874207609@qq.com |
引用文本:
lanlvdeng.ICP-OES测定低品位铬铁矿中Cr含量[J].中国无机分析化学,2019,9(6):45-48.
lanlvdeng.Determination of Chromium in Low-grade Chromite by Inductively Coupled Plasma Optical Emission Spectrometry[J].Chinese Journal of Inorganic Analytical Chemistry,2019,9(6):45-48.
lanlvdeng.ICP-OES测定低品位铬铁矿中Cr含量[J].中国无机分析化学,2019,9(6):45-48.
lanlvdeng.Determination of Chromium in Low-grade Chromite by Inductively Coupled Plasma Optical Emission Spectrometry[J].Chinese Journal of Inorganic Analytical Chemistry,2019,9(6):45-48.