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Analyses of elemental compositions of ctrontium-permanent magnetic ferrite by X-ray fluorescence spectrometry using a fusion method for sample preparation |
Received:August 22, 2010 Revised:December 26, 2010 |
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DOI:10.3969/j.issn.2095-1035.2011.01.0011 |
KeyWord:X-ray fluorescence spectrometry; permanent magnetic ferrite; iron;strontium;silicon |
Author | Institution |
ZHU Zemin |
北矿磁材科技股份有限公司,北京 |
DU Zhiguo |
北矿磁材科技股份有限公司,北京 |
JIANG Xueliang |
大连交通大学,大连 |
YAO Guiju |
北矿磁材科技股份有限公司,北京 |
CHEN Liqing |
北矿磁材科技股份有限公司,北京 |
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Abstract: |
This study demonstrated a novel analytical approach to determine concentration of Fe, Sr and Si elements in semi-finished products of permanent magnetic ferrite by X-ray fluorescence measurement. Samples were melted with bead and mixed melting reagents. Self-made synthetic standards were used for quantification analysis. Our results indicated that the minimum relative standard deviation of 0.1% could be achieved for the eleven parallel measurements, indicating high accuracy and good reproducibility for the analytical approach we developed and demonstrated in this study. It concluded that when analyzing real samples by XRF, the results were consistent with that of traditional chemical analysis methods. |
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