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Determination of Trace Bromate in Water by Precolumn Derivation- High Performance Liquid Chromatography (HPLC) |
Received:October 17, 2011 Revised:December 31, 2011 |
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DOI:10.3969/j.issn.2095-1035.2012.01.0005 |
KeyWord:bromated;pre-column derivation;high performance liquid chromatography;optimization |
Author | Institution |
LIU Zhen |
中国药科大学 分析化学教研室,江苏 南京 |
CUI Yan |
中国药科大学 分析化学教研室,江苏 南京;江苏正大天晴制药有限公司,江苏 南京 |
HU Zhijun |
中国药科大学 分析化学教研室,江苏 南京 |
CHEN Jianqiu |
中国药科大学 分析化学教研室,江苏 南京 |
YAN Zhenyu |
中国药科大学 分析化学教研室,江苏 南京 |
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Abstract: |
A new HPLC method associated with pre-column derivation technique was established to detect trace bromate in water. And the derivation conditions were optimized in this study. The recoveries of the method were in the range of 98% to 105% with the relative standard deviation of less than 1.9% (n=9). Its regression coefficient was 0.9995, and the limit of detection was 1.0 μg/L. This method is simple, fast and reliable, thus meet current requirement for testing a standard. |
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