Comparative Studies on the Fifteen Elements in the Black Beans and Small Red Beans by Inductively Coupled Plasma Atomic Emission Spectrometry(ICP-AES)
Received:April 11, 2013  Revised:April 26, 2013
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DOI:doi:10.3969/j.issn.2095-1035.2013.03.012
KeyWord:ICP-AES;black beans; small red beans;simultaneous determination
              
AuthorInstitution
ZHANG Guoyu 通辽市科尔沁区环境保护监测站,内蒙古 通辽
ZHAO Yuying 内蒙古民族大学 分析测试中心天然产物开发与废弃物利用研究所,内蒙古 通辽
ZHENG Qingfu 内蒙古民族大学 分析测试中心天然产物开发与废弃物利用研究所,内蒙古 通辽
SONG Juanjuan 内蒙古民族大学 分析测试中心天然产物开发与废弃物利用研究所,内蒙古 通辽
ZHOU Hong 内蒙古民族大学 分析测试中心天然产物开发与废弃物利用研究所,内蒙古 通辽
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Abstract:
      The contents of the fifteen elements, which include Na, Sn, Ca, Zn, Cu, Mg, Al, Fe, P, K, Si, Se, Ba, Mn, and Mo, in black beans and small red beans were simultaneously determined by the inductively coupled plasma atomic emission spectrometry (ICP-AES) method. In addition, the spiked recovery experiments were conducted for each element. The average recovery of each element in the black beans and small red beans are in the range of 93.11% to 102.15%. The RSDs are between 0.83% to 2.8% and the detection limits are in the range from 0.11 to 14.09 μg/L. A simple, rapid, accurate and stable testing method for the determination of the elements in the black beans and the small red beans has been established. The results showed that the contents of major elements and trace element in the black beans and small red beans, including K, Ca, P, Mg, Mn, Fe, Zn, etc., are relatively high. The contents of the nutrient elements, such as Ca, Mg, Fe , Zn, etc., are higher in the small red beans than that in the black beans.
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