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Determination of Nb、Sn、Fe and Cr#$NBSin N18 alloy by Inductively Coupled Plasma Atomic Emission Spectrometry |
Received:December 02, 2014 Revised:December 11, 2014 |
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DOI: |
KeyWord:N18 alloy; Nb; Sn; Fe; Cr; inductively coupled plasma atomic emission spectrometry |
Author | Institution |
yang jun hong |
西部金属材料股份有限公司 西安市 |
li tuo |
西部金属材料股份有限公司 西安市 |
SHI XIN CENG |
西部金属材料股份有限公司 西安市 |
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Abstract: |
A new method for determination of Nb、Sn、Fe and Cr in N18 alloy by inductively coupled plasma atomic emission spectrometry was established. The determined conditions such as the sample pre-treatment method, the matrix and the analytical lines were discussed in this paper. It was showed that interferences were eliminated by using the matrix matching method and the experimental conditions were optimal. The proposed method has been applied to determine the Nb、Sn、Fe and Cr in N18 alloy, the determination results were consistent with those obtained by chemical method. The recovery was 96.7%~101.0%, and the relative standard deviation (RSD, n=11) were less than 3.0 %. |
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