Development of Certified Reference Materials of Titanium Ore and Ilmenite Concentrate for X-ray Fluorescence Spectrometry & Chemical Analysis
Received:July 24, 2017  Revised:November 19, 2017
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DOI:doi:10.3969/j.issn.2095-1035.2018.01.006
KeyWord:titanium ore; ilmenite concentrate; certified reference materials (CRMs); X-ray fluorescence spectrometry;chemical analysis
                 
AuthorInstitution
WANG Xueying 山东众标企信检测科技有限公司,济南
WANG Feifei 济南众标科技有限公司,济南
SUN Xiaoxuan 济南众标科技有限公司,济南
LIU Kai 济南众标科技有限公司,济南
WANG Bingying 济南众标科技有限公司,济南
SI Zhenqi 济南众标科技有限公司,济南
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Abstract:
      The certified reference materials (CRMs) of titanium ore and ilmenite concentrate for chemical analysis and X-ray fluorescence spectrometry were developed. Samplesweretakenfrom different local and foreign representative mining sites. Multi-stage crushing and three-dimensional mechanical mixing process was adopted toprepare homogenized CRMs. For sixteen elements present in CRMs,standard values withuncertaintywereverified using standard analysis methods which shows good analytical stability of samples in the working line. These CRMs filled the gaps of national and international standard materials for XRF spectrometry and have been approved as national CRMs by State General Administration of P.R.China and Standardization Administration of the People’s Republic of China.
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