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Determination of Phosphorus in Rare Earth Phosphate Leaching Solution by Spectrophotometry |
Received:March 05, 2018 Revised:July 06, 2018 |
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DOI: |
KeyWord:Associated rare earth phosphate rock; leaching; Phosphorus; spectrophotometry |
Author | Institution |
yulili |
广东省资源综合利用研究所 |
肖飞燕 |
稀有金属分离与综合利用国家重点实验室;广东省资源综合利用研究所 |
wushifeng |
稀有金属分离与综合利用国家重点实验室;广东省资源综合利用研究所 |
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Abstract: |
In this paper, the determination of phosphorus in leaching solution of rare earth phosphate rock by ammonium molybdate spectrophotometry was studied.The effects of the amount of developer and the acidity of nitric acid on the determination of phosphorus were investigated by experiments. the accuracy and precision of the method were also investigated.The experimental results show that the precision of the method is good, the relative standard deviation is less than 3%. Compared with the gravimetric method for determination of phosphorus, the results of the two methods are consistent. The method can accurately detect the phosphorus in the leaching solution of the associated rare earth phosphate rock.It was a simple, rapid and accurate analytical method for investigating the leaching rate of phosphorus in the hydrometallurgical process of rare earth phosphate rock. |
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