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Determination of Arsenic and Mercury Content in Copper Matte by Microwave Digestion-ICP-AES |
Received:April 02, 2019 Revised:April 10, 2019 |
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DOI:10.3969/j.issn.2095-1035.2019.04.006 |
KeyWord:microwave digestion;inductively coupled plasma atomic emission spectriometry(ICP-AES); copper matte; arsenic; mercury |
Author | Institution |
lvqianqian |
铜陵有色金属集团控股有限公司检测研究中心 |
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Abstract: |
The sample of copper matte was treated by microwave digestion method. As 188.979 nm and Hg 194.227 nm were selected as the analytical lines. A determination method of arsenic and mercury content in copper matte was established by inductively coupled plasma atomic emission spectriometry(ICP-AES). The results showed that the sample of copper matte could be completely dissolved by this method. The detection limit for arsenic is 3.1 ug/g and for mercury is 0.7 ug/g. The method is simple and fast. The elements recoveries ranged from 95 % to 110 %,and the relative standard deviation was less than 4 %, this method could reach the determination requirements of arsenic and mercury content in copper matte. |
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