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Study on Automatic Solid Phase Extraction System to Separate Iron Isotope from Geological Samples |
Received:November 06, 2019 Revised:March 26, 2020 |
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DOI:doi:10.3969/j.issn.2095-1035.2020.03.017 |
KeyWord:Automated solid phase extraction system, Iron isotope, Separation and enrichment |
Author | Institution |
Xiang Mei |
成都理工大学 |
Wang Tong |
成都理工大学 |
Xu Jinyong |
成都理工大学 |
Shi Yajing |
成都理工大学 |
Ren Ziwei |
成都理工大学 |
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Abstract: |
An automatic solid phase extraction system was developed to separate iron from geological samples. The system has four parallel channels and can process four samples at a time. One extraction procedure will take 24 minutes for 4 samples. The iron was separated from granite (GBW07103)with AG1-X8 anion resin. Iron can be converted into anionicScomplex in 6 mol L-1 hydrochloric acid and adsorbed on AG1-X8 anion resin. While iron can be eluted with 8 mol L-1 Nitric acid and H2O. The recovery of iron was 96%-107%. It eliminates the influence of matrix, improves sample processing efficiency, reduces the risk of human contamination, and is a diversified sample processing tool. |
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