Study on Automatic Solid Phase Extraction System to Separate Iron Isotope from Geological Samples
Received:November 06, 2019  Revised:March 26, 2020
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DOI:doi:10.3969/j.issn.2095-1035.2020.03.017
KeyWord:Automated solid phase extraction system, Iron isotope, Separation and enrichment
              
AuthorInstitution
Xiang Mei 成都理工大学
Wang Tong 成都理工大学
Xu Jinyong 成都理工大学
Shi Yajing 成都理工大学
Ren Ziwei 成都理工大学
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Abstract:
      An automatic solid phase extraction system was developed to separate iron from geological samples. The system has four parallel channels and can process four samples at a time. One extraction procedure will take 24 minutes for 4 samples. The iron was separated from granite (GBW07103)with AG1-X8 anion resin. Iron can be converted into anionicScomplex in 6 mol L-1 hydrochloric acid and adsorbed on AG1-X8 anion resin. While iron can be eluted with 8 mol L-1 Nitric acid and H2O. The recovery of iron was 96%-107%. It eliminates the influence of matrix, improves sample processing efficiency, reduces the risk of human contamination, and is a diversified sample processing tool.
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