杨海娇,骆坤,赵永莉.电感耦合等离子体原子发射光谱(ICP-AES)法测定球化剂中镧、铈、钇[J].中国无机分析化学,2019,9(3):55-57.
电感耦合等离子体原子发射光谱(ICP-AES)法测定球化剂中镧、铈、钇
Determination of Lanthanum, Cerium, Yttrium in Nodulizer by Inductively Coupled Plasma Atomic Emission Spectrometry
投稿时间:2019-01-29  修订日期:2019-01-31
DOI:doi:10.3969/j.issn.2095-1035.2019.03.014
中文关键词:  ICP-AES  球化剂;稀土;镧;铈;钇
英文关键词:Inductively Coupled Plasma-Atomic Emission Spectrometry(ICP-AES)  Nodulizer  Rare Earth  Lanthanum
基金项目:
        
作者单位
杨海娇 共享装备股份有限公司检测中心
骆坤 共享装备股份有限公司检测中心
赵永莉 共享装备股份有限公司检测中心
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中文摘要:
      应用电感耦合等离子体发射光谱(ICP-AES)法对球化剂中镧、铈、钇进行测定,通过硝酸、氢氟酸和盐酸分解试料,高氯酸冒烟驱走硅和氟,最后用盐酸溶解盐类,此方法能准确、快速地测定其含量,回收率在97%~100%之间,精密度试验取得了满意的结果。
英文摘要:
      The sample was dissolved with nitric acid,hydrofluoric acid and hydrochloric acid,and processed with perchloric acid to remove silicon and fluorine,then the salts dissolved by hydrochloric acid.Determination of lanthanum,cerium,yttrium in nodulizer by the method of inductively coupled plasma atomic emission spectrometry(ICP-AES) was proposed.The content of the elements could be determined correctly and quickly.The recoveries obtained were in the range of 97% to 100%,the precision of the method was satisfacted.
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